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HH-Caproic acid填充柱 己酸的純度測定
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HH-Caproic acid填充柱 己酸的純度測定

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產(chǎn)品名稱:HH-Caproic acid填充柱 己酸的純度測定

產(chǎn)品型號:HH-Caproic acid填充柱

產(chǎn)品廠商:浩瀚色譜(山東)應(yīng)用技術(shù)開發(fā)有限公司

簡單介紹

己酸的純度測定,液化石油氣,二甲醚,甲縮醛,乙縮醛,乙醇,室內(nèi)空氣,焦?fàn)t煤氣,煉廠氣,天然氣,變壓器油,多氯聯(lián)苯,植物油,6號溶劑殘留,裂解進(jìn)樣器,消毒劑,氨水,乙縮醛

HH-Caproic acid填充柱 己酸的純度測定的詳細(xì)介紹

己酸的純度測定
己酸的純度測定 詳細(xì)信息:

名稱:填充柱
規(guī)格:2m*3mm
型號:HH-Caproic acid
應(yīng)用:己酸的純度測定


對己酸新的合成工藝進(jìn)行了探討。采用二步法制備已酸,以2-辛醇為反應(yīng)原料,2-辛醇?xì)庀嗝撍玫?-辛烯,再氧化2-辛烯為已酸的合成工藝路線;研究了負(fù)載型脫水催化劑對2-辛醇?xì)庀嗝撍铣?-辛烯的催化作用,由固定床反應(yīng)器考察了其催化性能;用XRD、BET等手段對催化劑進(jìn)行表征,研究其可能的反應(yīng)機(jī)理,并對催化劑的失活原因進(jìn)行了考察;以過氧化氫為氧化劑,磷鎢酸為催化劑,十六烷基吡啶為相轉(zhuǎn)移催化劑催化氧化2-辛烯制備已酸;分別考察了反應(yīng)溫度、反應(yīng)時間、催化劑的物質(zhì)的量對已酸收率的影響;研究了反應(yīng)控制相轉(zhuǎn)移催化劑的反應(yīng)機(jī)理,因?yàn)榇呋瘎┠芑厥?,這種氧化2-辛烯為已酸的合成方法更加環(huán)境友好和經(jīng)濟(jì)性。

滕州市浩瀚色譜儀器技術(shù)服務(wù)有限公司,研發(fā)專用填充柱測定己酸的純度,雜質(zhì)空氣,水分,辛醇和己酸得到有效分離,面積歸一法定量,結(jié)果準(zhǔn)確。

己酸的純度測定 測試譜圖:



Purity determination of caproic acid
Determination of the purity of hexanoic acid Details:

Name: Packed column
Specification: 2m*3mm
Model: HH-Caproic acid
Application: Purity determination of caproic acid


The new synthetic process of caproic acid was discussed. A two-step method was used to prepare hexanoic acid, with 2-octanol as the reaction raw material, 2-octanol gas-phase dehydration to obtain 2-octene, and 2-octene reoxidation as the synthesis process of hexanoic acid; The catalytic performance of 2-octanol gas-phase dehydration to 2-octene was investigated by a fixed bed reactor; the catalyst was characterized by XRD, BET and other means, and its possible reaction mechanism was studied, and the catalyst was deactivated The reasons were investigated; hydrogen peroxide was used as the oxidant, phosphotungstic acid was used as the catalyst, and cetylpyridine was used as the phase transfer catalyst to catalyze the oxidation of 2-octene to hexanoic acid; the reaction temperature, reaction time, and the catalyst material were investigated separately The influence of the amount on the yield of hexanoic acid; the reaction mechanism of the reaction control phase transfer catalyst is studied. Because the catalyst can be recycled, the synthesis method of oxidizing 2-octene to hexanoic acid is more environmentally friendly and economical.

Tengzhou Haohan Chromatography Instrument Technology Service Co., Ltd. has developed a special packed column to determine the purity of caproic acid. Impurity air, moisture, octanol and caproic acid are effectively separated, and the area normalization method is quantified, and the result is accurate and reliable.

Purity determination of caproic acid Test spectrum:

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