名稱(chēng)：毛細(xì)管柱
固定液：50%苯基甲基聚硅氧烷
規(guī)格：30m*0.53mm

型號(hào)：OV-17
應(yīng)用：GB/T 14552-2003 水、土中有機(jī)磷農(nóng)藥測(cè)定的氣相色譜法

浩瀚色譜（山東）應(yīng)用技術(shù)開(kāi)發(fā)有限公司提出了固相萃取分離-毛細(xì)管柱-氣相色譜法測(cè)定水中11種有機(jī)磷農(nóng)藥的方法。水樣經(jīng)固相萃取小柱分離并凈化,甲醇-丙酮(70+30)混合液洗脫。用OV-17色譜柱(30m×0.53mm)分離,脈沖火焰光度檢測(cè)器檢測(cè)。11種有機(jī)磷農(nóng)藥的質(zhì)量濃度均在5.00μg·L-1以?xún)?nèi)與其峰面積呈線(xiàn)性關(guān)系,測(cè)定下限(10S/N)在0.03~0.05μg·L-1之間。方法用于地表水樣和飲用水樣分析,加標(biāo)回收率在65.7%~124%之間,測(cè)定值的相對(duì)標(biāo)準(zhǔn)偏差(n=6)在1.8%~9.9%之間。


水、土中有機(jī)磷農(nóng)藥測(cè)定OV-17毛細(xì)管柱  測(cè)試譜圖：


Determination of Organophosphorus Pesticides in Water and Soil by OV-17 Capillary Column
OV-17 capillary column for the determination of organophosphorus pesticides in water and soil Details:

Name: capillary column
Fixative: 50% phenylmethylpolysiloxane
Specifications: 30m*0.53mm

Model: OV-17
Application: GB/T 14552-2003 Gas chromatographic method for the determination of organophosphorus pesticides in water and soil

Haohan Chromatography (Shandong) Application Technology Development Co., Ltd. proposed a method for the determination of 11 organophosphorus pesticides in water by solid-phase extraction separation-capillary column-gas chromatography. The water sample was separated and purified by solid phase extraction cartridge, and eluted with methanol-acetone (70+30) mixture. Separated by OV-17 chromatographic column (30m×0.53mm), detected by pulsed flame photometric detector. The mass concentrations of 11 organophosphorus pesticides were all within 5.00μg·L-1 and their peak areas were linearly related, and the lower limit of determination (10S/N) was between 0.03 and 0.05μg·L-1. The method was applied to the analysis of surface water samples and drinking water samples. The recoveries of standard additions were between 65.7% and 124%, and the relative standard deviations (n=6) of the measured values were between 1.8% and 9.9%.


Determination of organophosphorus pesticides in water and soil OV-17 capillary column Test spectrum: